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An agitated liquid liquid process involves many simultaneous, interdependent phenomena, such as dispersion, coalescence, suspension, heat and mass transfer, and chemical reaction. Previously described nitration requires control of the interfacial area rather than speci c drop size, but some processes require precise control of drop size. For example, equipment for suspension polymerization processes must be capable of producing uniform beads of speci ed size range as well as providing for heat transfer and drop suspension. Flow patterns and turbulence in stirred vessels are complex phenomena that can often be better appreciated using modern tools such as laser Doppler velocimetry (LDV), particle image velocimetry (PIV), and computational uid dynamics (CFD). All show turbulence consisting of high-energy eddies near the impeller, and lowerenergy eddies located farther away. Turbulence intensities near the impeller can be 40 times greater than the mean for the entire vessel. Turbulence intensities are very low in regions close to the wall and at the top and bottom of the vessel. Flow patterns are sensitive to impeller geometry, the number of impellers, and their position in the vessel. The reader is referred to s 2 and 6 for more detail. Since drop size depends on ow-dependent dispersion and coalescence phenomena, it can be concluded that certain regions of the vessel are dominated by dispersion while others are dominated by coalescence. When a drop is contained within a larger eddy, it rotates within that eddy and does not break up. However, if it encounters an eddy of its size or smaller, it can be deformed and dispersed. When drops suspended in gentle ows collide, they often remain in contact long enough to coalesce.

Description SQL error or missing database Internal logic error Access permission denied Callback routine requested an abort Database le is locked Table in a database is locked Out of memory (not used in the current version of Symbian SQL) Attempt to write to a read-only database Operation terminated by sqlite3_interrupt I/O error Database le image invalid Table or record not found Database is full Unable to open database le Database lock protocol error Database is empty Bad schema Too much data for one row Constraint violation Data type mismatch (continued overleaf )

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13-422 Scale-up of Liquid Liquid Reactions Despite the frequent need to run reactions in immiscible liquid systems, the reliability and applicability of correlations to predict drop size distribution and surface area of the dispersed phase, especially in the presence of reactions, is limited The reader is referred to 12 and Section 13-35 This problem is due in part to effects that small changes in physical aspects such as small agitator blade width can have on dispersed phase drop size as well as on surfactant effects resulting from reacting substrates It is sometimes even dif cult to predict which phase will be continuous and which dispersed Although this factor is normally a property of a given system, it can sometimes be reversed by the manner in which the phases are contacted (ie, by mixing during addition as opposed to starting with both phases present).

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Extreme care must be taken during laboratory and piloting studies to determine the extent to which interfacial differences are signi cant so that the impact of changes in dispersion that are very likely to occur on scale-up can be evaluated In many cases these changes may not be signi cant because other aspects of the reacting system are controlling However, phase dispersion can be critical to selectivity in some cases because of complex interfacial interactions Selection of impellers and speeds to achieve the desired drop size distribution (which has a direct effect on settling rate) can also be critical to reactions that require subsequent phase separation The uncertainties inherent in scale-up of liquid liquid systems, especially if selectivity is affected, require testing over a wide range of operating conditions in the laboratory and possibly the pilot plant to determine the sensitivity of each system to changes in dispersion characteristics.

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