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8.4.7 ANALYTICAL METHODS The aim of validation of an analytical procedure is to demonstrate that the method employed in any product testing, such as the identi cation, control of impurities, assay, dissolution, particle size, water content, or residual solvents, is validated in the most important characteristics. Identi cation tests, quantitative tests for impurities content, limit tests for control of impurities, and quantitative tests of the active moiety in samples of pharmaceutical product are the most common types of analytical procedures that validation addresses [1]. However, other analytical procedures, such as dissolution testing for dosage form or particle size determination for drug substance, are required for validation of analytical procedures. The revalidation of an analytical procedure is possible when, in particular circumstances, it could show changes in the synthesis of the drug substance, the composition of the nished product, or the analytical procedure. However, certain other changes may require validation as well. Method validation should con rm that the analytical procedure employed for a speci c test is suitable for its intended use. The validation of an analytical method

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The FDA has stressed that the release of the pharmaceutical QS guidance document does not impose new regulatory requirements on manufacturers but encourages manufactures to adopt a quality systems approach to cGMP compliance because of the potential bene ts. An appropriately designed and implemented quality system can do the following:

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[14] Y Xuan, CM Snowden, A generalised approach to the design of microwave oscillators , IEEE Trans Microwave Theory Tech, 35(12), 1340 1347, 1987 [15] Y Xuan, CM Snowden, Optimal computer-aided design of monolothic microwave integrated oscillators , IEEE Trans Microwave Theory Tech, 37(9), 1481 1484, 1989 [16] Y Mitsui, M Nakatani, S Mitsui, Design of GaAs MESFET oscillator using large-signal S-parameters , IEEE Trans Microwave Theory Tech, 25(12), 981 984, 1977 [17] EW Bryerton, WA Shiroma, ZB Popovic, A 5-GHz high-ef ciency class-E oscillator , IEEE Microwave Guided Wave Lett, 6(12), 441 443, 1996 [18] M Prigent, M Camiade, G Pataut, D Reffet, JM Nebus, J Obregon, High ef ciency free running class-F oscillator , IEEE MTT-S Int Symp Dig, 1995, pp 1317 1320 [19] V Rizzoli, A Costanzo, A.

Adobe completely revamped the type tool in Photoshop 6, as I mentioned earlier. The following steps show you the basics of using the new tool and its accompanying options. Note that these steps assume that you re creating text for the first time in your image (more about adding to existing text later).

One of the great things about DDR and DDR2 modules is that later ones are backward compatible (as long as the number of pins matches). So, a board that can take PC-2100 modules is also compatible with PC-2700 and PC-3200, and a board that is compatible with PC-2700 will also be able to work with PC-3200 (but not PC-2100). The same is true for DDR2, although DDR and DDR2 modules aren t interchangeable (there s no danger of doing this by accident because the number of pins is completely different).

Neri, Harmonic-balance analysis of microwave oscillators with automatic suppression of degenerate solution , Electron Lett, 28(3), 256 257, 1992 [20] CR Chang, MB Steer, S Martin, E Reese, Computer-aided analysis of free-running oscillators , IEEE Trans Microwave Theory Tech, 39(10), 1735 1745, 1991 [21] BD Bates, PJ Khan, Stability of multifrequency negative-resistance oscillators , IEEE Trans Microwave Theory Tech, MTT-32, 1310 1318, 1984 [22] V Rizzoli, A Costanzo, C Cecchetti, Numerical optimisation of microwave oscillators and VCOs , IEEE MTT-S Int Microwave Symp Dig, 1993, pp 629 632 [23] V Rizzoli, A Neri, Harmonic-balance analysis of multitone autonomous nonlinear microwave circuits , IEEE MTT-S Int Microwave Symp Dig, 1991, pp 107 110 [24] KKM Cheng, JKA Everard, A new and ef cient approach to the analysis and design of GaAs MESFET microwave oscillators , IEEE MTT-S Int.

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